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By Bancroft W. D.

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T. Murakawa, Y. Kono, M. Nishida, S. Goto and S. Kuwahara, Chemotherapy (Tokyo), 21, 1399 (1973); Chem. , 84, 53721 (1973). 187. RN. M. S. Avery, Drugs, 9, 88 (1975). 188. A. McK. Bennett, The Use of Antibiotics, 4th edition, Heinemann, Oxford, 172 (1987). 189. R N . Brogden, R C . M. S. Avery, Drugs, 18. 169 (1979). 190. A. Todd and P. Beniield, Drugs, 39,264 (1990). 191. F. Westphal, A. M. Brogard and C . Carbon, J. Antimicrob. , 27,647 (1991). 192. F. E. C. C. Aristorena, L. M. Pla-Delfina, Biophurm.

Measurement of this was used as the assay method in the 1973 British Pharmacopoeia [75]. The product was 33 ALBERT E. BIRD thought to be the penicillenic acid of amoxicillin, X, R=NH, [ 11, but this is unlikely because this compound is expected to be unstable due to faciie reaction of the amino group with the oxazolone ring [76]. This is supported by failure to obtain the penicillenic acid by reaction with imidazole and mercuric chloride under conditions which gave a stable penicillenic acid suitable for assay purposes from penicillins without an a-amino group [77].

E. Roets, P. De Pourcq, S. Toppet, J. Hoogmartens, H. H. J. Smith, J. , 303, 117 ( 1984). 49. J. Haginaka and J. Wakai, Chent. Pharm. , 34,2239 (1986). 50. G. De Angeli, G. Mercandalli, F. Minoja, S. Cingolani, I / Farmaco Ed. , 35, 100 (1980). 5 1. E. R. C. Marshall, J. Pharm. , 38,9 13 ( 1986). 5 2 . F. Moll and A. Esperester, Arch. , 312, I054 (1979). 53. M. E. L. Engel, J. Pharm. , 33, 119 (1981). 54. T. Uno, M. Masada, Y. Kuroda and T. Nakagawa, Chem. Pharni. Bull. 29, 1344 (1981). 5 5 . P.

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Activation by Charcoal by Bancroft W. D.


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